MEEG 655/855: Principles of Composites Manufacturing

Assignment no:1

Due Date:  Lecture4 (Sept. 8th)

I: Answer in one to two sentences
1.What are the two major ingredients of a composite material? What characteristics of these ingredients enhance the properties of the composite material?

 2.Is it easier to inject a thermoplastic or thermoset resins through a tightly knit fiber preform? Why?

3.Which one of the following has more influence on the mathematical modeling of the manufacturing process: (a) the fiber material (e.g., glass or carbon), or (b) whether the fibers are discontinuous or continuous? Why?

4.List the main differences between thermoplastic and thermoset resins that influence their processing?

5.What is the difference in terms of flow modeling between short fiber composites, thermoset matrix advanced composites and thermoplastic matrix composites?

6.List critical issues in injection molding process. What important physics you would have to consider formulating a model to address these issues?

7.What is the major difference between Injection Molding and Extrusion?

 8.What are some of the advantages and disadvantages of compression molding as compared with injection molding?

 9.What do you understand by precursor material? Provide sketches of five of them and mention the processes in which they are used.

10.List important transport and critical issues in thermoset filament winding, autoclave processing and liquid composite molding. Name at least two issues that are common to all the thermoset processes listed above and name at least one issues that is specific to each individual process.

  II.You have been asked to select a composite manufacturing process due to your familiarity with the processes as a result of the course you took at the University of Delaware. Your company is considering the option to make the following 5 components and would like you to recommend which process should be considered with a single sentence explanation as to why you selected that process.

1.Short fiber reinforced dashboards for the new Acura car.

2.Telephone poles for the city of Newark

3.I-beams with complex curvatures for Ford Passenger Vans

4.Axi-symmetric casing for the rocket motor

5.Recycleable door panels for the Mercedes Benz.

III. Composite materials are replacing traditional materials in many applications. List at least 10 examples of composite material use in different applications. Also state the reason for the replacement. Can you think of a component or an application that is currently not being made of composite materials but will benefit greatly if it was ?


MEEG 655 PRINCIPLES OF COMPOSITE MANUFACTURING PROCESSES
ASSIGNMENT # 2
Due: Sept 27th, 2005
1. Flow through a circular tube (20%)

Resin of viscosity 1 Poise is made to flow through a tube of radius R from a bucket at atmospheric pressure by applying a perfect vacuum at the other end. The length of the tube is L.
(a) Calculate the steady state flow rate of the resin through the tube if R= 4 mm and L= 30 cm.
(b) Now if you attach a second tube of R= 2mm and L= 30cm at the end of the first tube through an air tight fitting, by what percentage will the flow rate reduce by as compared to the flow rate in part (a)?

2. PERMEABILITY CHARACTERIZATION EXPERIMENT (80%) (outreach students- skip this problem)

The goal is to find the permeability of a glass fabric in one of its principal directions. The permeability characterization experiment will be performed for a selected fiber volume fraction with the fluid being injected under constant injection pressure. A video camera will record the visible flow front progression through the transparent mold lid. A scale may be placed along the mold length to later extract the information of location of the flow front as a function of time

Steps in the procedure

·Partially assemble the mold
·Carefully cut the fabric layers
·Stack the fabric layer in the mold cavity
·Close the mold
·Prepare the corn syrup and water mixture and measure its viscosity (should be in the range of 50 to 500 cp) ( one cp is the viscosity of water)
·Place the fluid in the container and pressurize it.
·Inject the fluid into the mold with constant pressure at the inlet
·Record the motion of the flow front with the camera
·Stop the experiment when the fluid reaches the vent
·Dismantle the setup
·Clean-up the mold and the area
·Process the data to find the permeability

MATERIAL AND PROCESS INFORMATION

Reinforcement material:Fiberglass

Random Mat

Density: 2570 kg/m3

Aerial weight: to be measured

Number of layers: 2

Mold: Cavity thickness: 3.2 mm

Width: 206.4 mm

Resin system:Mixture of corn syrup and water

Viscosity: to be measured

Injection pressure to be obtained during the experiment: 10-15 psi (Please DO NOT exceed)

I.Measure the aerial weight of the preform used and deduce its porosity value for the experiment using the dimensions of the mold

II.Conduct the experiment in a group of 3 or 4 and save the data collection video of the experiment (bring a memory stick or a zip disk)

III.Find the permeability of the preform for the fiber volume fraction you used. Show all your calculations on how you obtained the permeability value. List possible errors in your experiments and recommend how you would improve the experiment. The group can share the experimental data but the report should be written individually

Outreach students only do Problems II and III not for in-class students!

II. Consider unidirectional stretching of a cylinder as shown in the figure below. At any time, t, assume that R(t) is independent of z. 

(a) Using only the conservation of mass show that the velocity field is given by
   uz  =  U *z/L(t)        and ur = - U *r/2*L(t)

b)   find the components of the strain rate tensor

c) Neglecting surface tension and inertia, calculate the force F required to pull the Newtonian Viscous cylinder.


 

 III. A layer of fluid with thickness d (delta)  flow down  a vertical wall as shown below. Gravity acts to pull the fluid down the wall.

 a.Find and sketch the velocity distribution for a Viscous Newtonian fluid of viscosity m (mu).
b. If you can measure the flow rate, what will be its thickness d (delta) in terms of viscosity and the flow rate Q
 
 


 

MEEG 655 PRINCIPLES OF COMPOSITE MANUFACTURING PROCESSES
ASSIGNMENT # 3
Due: Sept 29th, 2005
Use of LIMS simulation to Locate Best Gate and Vent Combination for the geometry assigned to your group. Each student should work independently and submit their own work
(1) For the assigned geometry to your group, use the LIMS program to find the best gate and vent combination that will lead to minimal void content. Report the void area and the time to fill (until the flow reaches the vent). Use the fiber volume fraction, viscosity and the permeability value from your permeability experiment that your group performed last week.
(2) For the same geometry introduce race tracking along all the edges in the mold where the fiber preform has to be flushed against a mold wall by doubling the bulk permeability value that you had assigned in (1) only for these edge elements. Re-run the simulation with the selected gate and vent and note the void fraction and fill time. Can you find a better gate and vent combination for this scenario
(3) For the same geometry, make the race tracking permeability 10 times higher than the bulk and report the results for the gate and vent combination of (1) and (2). Is there a gate and vent combination that is better than (1) and (2) for this case?
(4) Discuss the implication of your results in a manufacturing environment and suggest your ideas of how one could reduce or use race tracking to one’s benefit.
Submit your assignment electronically with figures that show the final filling scenario for each case by Sept. 29th, 2005
Automotive fender:
Automotive hood:
Window frame:
Multiple insert geometry:
 
Full rectangle geometry:
 


Notes:
· You can check the E-Calc lab schedule at this website:
o http://www.engr.udel.edu/eCALC/
· In the class folder (_MEEG655_fall05), is a power point file summarizing the information presented on how to use LIMS. The end of this document contains specific info on simulating the vent effects.
· An additional power point file in the Assignment sub-directory shows all of the 5 geometries with the gate and vent node numbers listed.
· You can set a gate by specifying the node number by selecting the node … select by number menu.
 
 

MEEG 655 PRINCIPLES OF COMPOSITE MANUFACTURING PROCESSES
ASSIGNMENT #4
Due: Oct 20th, 2005


    I.Heating of a composite between two aluminum plates

Consider a glass-polypropylene composite 0.3 cm  thick  at room temperature of 25C to be heated by conduction by  aluminum platens  held at 150C.

   1. How long will it take for the midplane of the glass-polypropylene composite containing 50% glass fibers to reach 125C?.
   2.If the composite contained 50% carbon fibers instead of glass fibers, how long would you wait until the center reaches 125C?.
   3.If these composites were placed in an oven at 200C, estimate the time  it would take to heat the composite to 175C. Assume the heat
     transfer coefficient between the air and the composite is 5 W/mK (For glass and Carbon properties please check the web/library/text)
 

II. Viscosity Measurements:
Below you are given some of the measurements made using a cone and plate viscometer of the torque and angular velocities. The radius of the plate is 1 cm and the angle of the cone is 9 degrees (pi/20)

         Torque (N-m)             angular Speed (rad/s)
         2.08E-05 0                    .015707963
         2.08E-04                        0.157079633
         6.53E-04                         1.570796327
         2.12E-03                         15.70796327
         6.47E-03                         157.0796327
 

   a.Find the two parameters if one were to use a two parameter power-law model
  b.Using the power-law model determine the pressure drop required to pump this material at a flow rate of 100 cc/s through a circular tube of radius 1 cm that is one meter long.
c. What would be your calculation for the pressure drop if you had assumed the fluid to be Newtonian?

III. Squeeze Flow with Slip Boundary Condition

     Consider a polymer being squeezed between parallel disks. The disk surfaces are lubricated so that there is a slip boundary condition
     in the radial direction. Assume inertia and body forces are negligible. Here H<< R and s =dH/dt

      a. Find velocity distribution
      b. Stresses and pressure in the fluid
      c. Find the total force exerted on the upper disk exerted by the fluid.

 

MEEG 655 PRINCIPLES OF COMPOSITE MANUFACTURING PROCESSES
ASSIGNMENT #5
Due: Nov 15th, 2005


I. The objective is to non-dimensionalize and simplify the following energy equation for the case of flow of a viscous thermoplastic Newtonian suspension in a cavity of length L, width W and thickness h by injection molding. The initial temperature of the melt coming into the mold is Ti and the wall temperature of the cavity is Tw. The injection of the material is done under a constant flow rate of Q cc/s. The thickness h << L and W. Assume that   is zero.

a. Identify independent and dependent parameters
b. Choose characteristic values to non-dimensionalize these parameters
c. Non-dimensionize the equation assuming that only shear stresses are important
d. Identify two important non-dimensional numbers (Brinkman number: measures the role of viscous dissipation compared to conduction, and Peclet number which measures the heat convected in the axial direction compared to the heat conducted in the transverse direction)
e. For small Pelcet number and uniform flow and heat transfer in the width direction, state the non-dimensional governing equation from part (d)
f. Find the steady state non-dimensional temperature solution for Brinkman number of  1, 10 and 100 and plot the temperature profile through the thickness.
 
 

II. Consider injection molding of a plaque 1 meter long, 50 centimeters wide and  0.25 centimeters thick. The injection is at one end of the plaque all along the width as shown in the figure below.

Two different plaques are to be manufactured. First one will contain polypropylene with 25% glass fibers which has an effective viscosity of 100 Poise and the second one contains nylon with 30% carbon fibers which has an effective viscosity of 1000 Poise. The mold wall is held at 25C. The polypropylene melt temperature is 175C and that of Nylon is 250C. The effective thermal conductivity of polypropylene with 25% glass is k= 1W/mC and that of Nylon with 30% carbon fibers is 10 W/mK. The injection rate is held constant at 100 cc/sec.
a. Find the approximate frozen layer thickness assuming fully developed flow away from the injection gate and the flow front for both, polypropylene and nylon
b. Find the maximum pressure that will be required approximately to fill the both the polypropylene and the nylon plaque.
c. If your marketing dept. wants to reduce the thickness of the plaque by half, how much pressure will the injection molding machine have to generate to fill the plaque under the same flow rate conditions?
 

MEEG 655 PRINCIPLES OF COMPOSITE MANUFACTURING PROCESSES
ASSIGNMENT #6
Due: Nov 29th, 2005
     I A screw extruder is 50 mm in diameter, 1 m long, has a 50mm lead, a channel 5 mm deep and a flight 3 mm wide. It is used to
     pump a fluid with ? = 5 x 105 poise and operates at a screw speed of 50 rpm.

     a. What is the maximum possible flow rate of the extruder under the circumstances ? What is the maximum possible pressure ?

     b. A die is attached to the end of the extruder, for which flow rate, is given as
     Q = K?P/?,
     where K=8.5 x 10-5 cm2. What flow rate and pressure result ?

     c. Does the  flow rate and pressure  in Part  (b) change if the viscosity increases ?

II.. Consider impregnation of fibertows as shown in figure 1.

The goal is to find the time it would take to impregnate a fiber tow of radius Ro. We can model this as flow through porous media with some reasonable assumptions. First, we can assume that capillary forces are negligent (pc=0). Second, we can assume that air trapped inside does not impact a back pressure on the resin (pin=0) and we can assume that the tow is symmetric and round and that Pout is constant on the outside as shown in figure 2.

 

Show that the time to fill this tow will be given by

Where delta P= Pout –pin, K is the permeability of the fiber tows in the radial direction, eta is the viscosity of the thermoplastic material and Vf is the fiber volume fraction inside the tow.

Calculate what fiber tow size you should ask the manufacturer of prepregs to use, if the viscosity of the resin is 1000 Pa.s , K is and fibers are packed in hexagonal arrangements inside the tow and you want to fill it in less than 100 seconds. The maximum pressure you can generate inside the mold is 100 MPa. Justify your analysis and your answer. Do you think your answer is a conservative one considering all the assumptions you have made?